PDF Ebook The Analytical Chemistry of SiliconesFrom Wiley-Interscience
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The Analytical Chemistry of SiliconesFrom Wiley-Interscience
PDF Ebook The Analytical Chemistry of SiliconesFrom Wiley-Interscience
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High-Resolution Solid-State NMR of Silicates and Zeolites Gunter Engelhardt and Dieter Michel "I strongly recommend this book as an important reference for scientists concerned with the structural properties of siliceous materials." --Applied Spectroscopy This well-organized and up-to-date text gives a thorough account of the wide range of applications of multinuclear high-resolution solid-state NMR spectroscopy in silicate and zeolite science, with emphasis on the kinds of chemical information retrievable from NMR experiments. 1988 (0 471-91597-1) 485 pp. The Chemistry of Silica Solubility, Polymerization, Colloid and Surface Properties, and Biochemistry Ralph K. Iler A major component of the earth's solid surface and the constituent of sand, silica--an ageless natural staple--is also integral to industries as diverse as chemistry, biology, medicine, agriculture, metallurgy, and mining. This landmark reference details the chemistry surrounding the research and development of silica as well as information on its production and production control. 1979 (0 471-02404-X) 866 pp. The Chemistry of Organic Silicon Compounds Parts 1 and 2 Edited by Saul Patai and Zvi Rappoport "This volume will probably become the first reference consulted for C-Si chemistry." --Choice This authoritative account of organic compounds containing carbon-silicon bonds brings specialists up-to-date to the field's latest innovative turns. The emphasis in this compilation of studies--from 17 prominent researchers--is on small molecules, single bonds, analysis, structure, synthesis, spectroscopy, and reaction mechanisms. Part 1:1989 (0 471-91441-X) 892 pp. Part 2:1989 (0 471-91992-6) 1,668 pp.
- Sales Rank: #2027534 in Books
- Published on: 1991-01-18
- Original language: English
- Number of items: 1
- Dimensions: 9.39" h x 1.42" w x 6.28" l, 2.09 pounds
- Binding: Hardcover
- 576 pages
From the Publisher
The fast paced developments in the field of silicone analytical chemistry over the last 15 years have been tremendous, and the explosion of knowledge during that time has been phenomenal. Updates the latest findings in the field and presents them in a concise, yet comprehensive manner. Principles and general approaches to problems are stressed, and examples cited of some of the typical approaches to problems of current interest, including: polymers and compositions; trace analysis; personal care applications; chromatographic methods; infrared, Raman, near-infrared and ultraviolet spectroscopy; nuclear magnetic resonance spectroscopy; mass spectrometry; and more. In addition, key references are cited for further reading.
From the Inside Flap
The new universe of innovative analytical techniques in chemistry—Fourier transform spectroscopy, near-infrared spectroscopy, a variety of surface analysis techniques, chemometrics and computerized instrumentation—has been matched in innovative velocity only by the phenomenal rise in uses for organosilicon materials. Indispensable as high-performance materials in industrial processes and products and in medical and biological applications, silicones offer a versatile new language for chemistry—whose syntax is understood through analytical technology. The Analytical Chemistry of Silicones is a guide to understanding the unique chemistry of organosilicon materials—a valuable compendium for chemists and engineers that covers techniques for analyzing, and analyzing for, organosilicon compounds. By frequently illustrating approaches with problems of current interest, the authors provide the reader with an up-to-the-minute glimpse into silicone chemistry’s full structural and analytical permutations. Inside, readers will find:
- Methods of analyzing for silicones —from parts per billion to 100%, both in bulk materials and on surfacesAnalysis of products and formulations—from coatings and cosmetics to surfactants and textile treatmentsAnalysis for traces of silicones—in foods, soil, water, air, medical devices, and biological samplesProven methods for analyzing organosilicon monomers and polymers for composition and structureExperimental methods for determining physical properties and polymer structureMicroscopical characterization techniques—from optical to analytical electron microscopyChromatographic, NMR, IR, mass spectrometric, atomic spectroscopic, and X-ray methods, and other key techniques—with emphasis on their uses in characterizing siliconesUp-to-date tables of physical property data for many monomers and oligomers, GC response factors, IR group frequencies, and NMR shiftsA comprehensive bibliography of relevant literature citations, including titles
From the Back Cover
High-Resolution Solid-State NMR of Silicates and Zeolites Günter Engelhardt and Dieter Michel "I strongly recommend this book as an important reference for scientists concerned with the structural properties of siliceous materials." —Applied Spectroscopy This well-organized and up-to-date text gives a thorough account of the wide range of applications of multinuclear high-resolution solid-state NMR spectroscopy in silicate and zeolite science, with emphasis on the kinds of chemical information retrievable from NMR experiments. 1988 (0 471-91597-1) 485 pp. The Chemistry of Silica Solubility, Polymerization, Colloid and Surface Properties, and Biochemistry Ralph K. Iler A major component of the earth’s solid surface and the constituent of sand, silica—an ageless natural staple—is also integral to industries as diverse as chemistry, biology, medicine, agriculture, metallurgy, and mining. This landmark reference details the chemistry surrounding the research and development of silica as well as information on its production and production control. 1979 (0 471-02404-X) 866 pp. The Chemistry of Organic Silicon Compounds Parts 1 and 2 Edited by Saul Patai and Zvi Rappoport "This volume will probably become the first reference consulted for C-Si chemistry…" —Choice This authoritative account of organic compounds containing carbon-silicon bonds brings specialists up-to-date to the field’s latest innovative turns. The emphasis in this compilation of studies—from 17 prominent researchers—is on small molecules, single bonds, analysis, structure, synthesis, spectroscopy, and reaction mechanisms. Part 1:1989 (0 471-91441-X) 892 pp. Part 2:1989 (0 471-91992-6) 1,668 pp.
Most helpful customer reviews
0 of 0 people found the following review helpful.
THE Standard for Silicone Analysis
By Moshe Dolejsi
This book is an absolute necessity if you work with any silicone based polymer and want to analyze it. Contains instructions on how to prepare samples, and how to conduct and interpret data from: HPLC, GC, MS, H-NMR, C-NMR, Si-NMR, and pretty much any technique you could think of. "But wait," you say, "I don't do work with PDMS, how useful will this be for me?" Great news for you then because the book also covers analysis of silicones containing aromatics, vinyls, halides, and whatever else you could think of. Different end caps? Yep. Small molecular weights? Yep. Large molecular weights? Yep. Not only does it have all this information but it also includes example spectra for most materials from every technique it covers. A few of them come from published literature and some comes from in house data collected by DOW Corning. Which brings me to my last point. Every author in this collection is from DOW Corning (Straight out of Midland). If anyone knows silicones it is DOW Corning, and if you want apply that knowledge to analyze your own samples this is the way to do it. In fact this book is really the only way to do it short of actually getting a job at DOW Corning (where I have no doubt they will probably also refer you to this book). If you have this book and don't agree with me, send me a message because the University library reclaimed my copy and I would be all to happy to get my own.
Long story short, if you work with silicones and want to obtain and interpret data from your samples your lab should have this book.
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